Programmable Advanced ECR - 2025-AS-01A-EN
Programmable Advanced ECR - 2025-AS-01A-EN

Programmable Advanced ECR - 2025-AS-01A-EN

Technical Specifications

Keithley 2450 – Quick Technical Highlights

  • 10 GΩ input impedance
    • Ideal for very high/low resistance samples with minimal loading.
  • Voltage or current sourcing for resistance
    • Safer and higher fidelity of measurement for high and low resistance samples
      • For high-resistance samples:
        • Using voltage sourcing gives a stable, noise-free drive signal. A controlled V-source avoids tiny current fluctuations that would corrupt the measurement.
      • For low-resistance samples:
        • Using current sourcing avoids voltage-burden and lead-resistance errors. A constant I-source gives a more accurate reading of very small resistances.
  • Adjustable voltage & current limits
    • Improves stability and protects the Device Under Test (DUT).

Core Performance Specs

  • Voltage range: ±200 V
  • Current range: ±1 A
  • Max output power: 20 W
  • Lowest voltage range: 20 mV
  • Voltage resolution: down to 10 nV
  • Current resolution: down to 10 fA
  • Lowest current range: 10 nA source, sub-nA measurement
  • Typical accuracy: ~0.012% (voltage & current)
Please read the General Presentation of ECR prior to reading this manual to understand the basics of ECR measurement.

General Presentation

Keithley 2450 with specificities highlighted. In dashed lines, parts for information only, not to be modified. In full line, parts susceptible to modifications
Keithley 2450 with specificities highlighted. In dashed lines, parts for information only, not to be modified. In full line, parts susceptible to modifications
The Keithley 2450 is composed of:
  • Output status: The ON/OFF button will be lit up when source output is on.
  • Sense probes: The terminal connections measure the voltage difference between the red and black probe. This measurement of the voltage drop on the DUT is done independently from the current sourcing.
  • Force terminals: The terminal connections are used to source current to the device under test (DUT).
  • Keithley ground: The terminal can be used to connect the ground of the Keithley to the instrument.
  • I/O Power Switch: Turns the instrument on or off. The instrument in on when the button is pressed down.

Programmable Advanced ECR Measurement

To realize an ECR measurement, you find need to configure the software to properly communicate with your Keithley.
Turn on the Keithley, start the instrument, the software and then go to the Configuration tab.
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Activate your Keithley under the Corrosion tab by selecting “Keithley” in “Type” and your specific Keithley in “Options”.
Configuration Window with Keithley selection
Configuration Window with Keithley selection
Once it is done, the software will restart, if the status shows an error message under “Initializing Keithley”, verify that the Keithley is ON and that the communication cable between the PC and the Keithley is properly connected.
Keithley 2450 ECR Measurement activation
Keithley 2450 ECR Measurement activation
It is only possible to activate an ECR measurement in a Standard step. To do so, go under the “Corrosion” tab and change the action from idle to any other option.
The options are custom SCPI commands which we will introduce later. To modify those options, you need to go back to the Configuration window and click on “CONFIG” next to the Keithley selected. The following window will appear:
Config window of Advanced ECR
Config window of Advanced ECR
  1. Commands Window:
      • CustomCmd(1/2/3/4): To modify the content of the command sent, you need to modify the content of “CustomCmd(1/2/3/4)”.
      • CC(1/2/3/4)Display: To modify the name that appears during the recipe creation, you need to modify the content of “CC(1/2/3/4)Display”.
  1. Commands Update:
      • Write and Read: If you enter a command on a line of the “Write” Column, by pressing “Write”, then “Read”, the line in the “Read” column will be automatically updated.
The command sent to the instrument can be customized based on the requirements of the tests. The next part will explain how to customize the commands to fit your requirements.

Programmable Advanced ECR Command control

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When setting a range, you should first set the limit to a value higher than the measure range you intend to set.
  • For most samples: Set the measure function to resistance. When the measure function is set to resistance, the instrument sets the source current and source values automatically.
  • For high resistance samples: Control voltage, measure current, and set measure units to ohms.
  • For low resistance samples: Control current, measure voltage, and set measure units to ohms.

Measure resistance using resistance function

When the measurement function is set to resistance, the Model 2450 measures resistance by sourcing current. The instrument automatically sets the magnitude of the current source, voltage limit, and the measure range.
This is the easiest method to measure resistance of the device under test and can be used in most cases.
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To select this type of measurement, click on “AUTO Resistance”.
The SCPI Command of the auto resistance does not need to be modified.
  • AUTO Resistance - 2Wire: One cable to the upper sample, one to the lower sample. Less precise measurement.
  • AUTO Resistance - 4Wire: Two cables to the upper sample, two to the lower sample. Less precise measurement.

Controlling current, measuring voltage, and reading in ohms

This measurement method is useful for low resistance samples.Low-resistance materials allow more current to pass easily. A higher current ensures accurate resistance measurements without excessive voltage drops.
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To select this type of measurement, click on “CONTROL Current”.
The SCPI Command of the CONTROL Current needs to be modified.
The user needs to replace the 3 dots with the desired parameters.
SOUR:CURR ...➔ Sets the sourcing current (in Amps)
SOUR:CURR:VLIM ➔ Sets the voltage limit (in Volts)
If you need any additional information regarding the other parameters in the SCPI commands, please contact your Rtec-Instruments representative.

Controlling voltage, measuring current, and reading in ohms

This measurement method is useful for high resistance samples.High-resistance materials allow only small currents to flow. Applying a higher voltage ensures you get a measurable current, improving signal-to-noise ratio.
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To select this type of measurement, click on “CONTROL Voltage”.
The SCPI Command of the CONTROL Voltage needs to be modified.
The user needs to replace the 3 dots with the desired parameters.
SOUR:VOLT ➔ Sets the sourcing voltage (in Volts)
SOUR:VOLT:ILIM ➔ Sets the current limit (in Amps)
If you need any additional information regarding the other parameters in the SCPI commands, please contact your Rtec-Instruments representative.

Measurement reading

Once the ECR measurement wiring is done and the appropriate resistance measurement method has been selected in the recipe, you can add the Keithley Resistance reading in “Data Logging”.
To select the 4 Wire Measurement reading, click on “OHM4W”.
If the resistance reading has been properly selected, it should appear in the “Run” tab.
Please refer to the General software manual for further explanations regarding the “Data Logging” and “Run” windows.